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Síntese de 1h-1,2,3-triazol-4-il-1,3,4-oxadiazóis a partir de 4-alcóxi-1,1,1-tricloro-3-alquen-2-onas
(Universidade Federal de Santa Maria, 2014-09-12)
This work describes the synthesis and the characterization of series of substituted trichloroacetyl 1H-1,2,3-triazoles (10 12), 1H-1,2,3-triazol-4-yl-carbohydrazides (14 16) and 1H-1,2,3-triazol-4-yl-1,3,4-oxadiazoles ...
Obtenção quimiosseletiva de trialometil-β-dicetonas via reações de acilação de acetais
(Universidade Federal de Santa Maria, 2009-02-27)
This work presents an Acylation Method of Acetals applied to the quimioseletive obtention of trifluormethyl-β-diketones, incluing acetals derived from not symmetrical ketones and functionalized substituents. Five known ...
Obtenção regiosseletiva de 5-alquil(aril/heteroaril)-3- (carboxil/trifluormetil)-1h-1-fenilpirazóis
(Universidade Federal de Santa Maria, 2011-05-19)
This paper presents a new synthetic route for obtain regioselective 5-alkyl(aryl/heteroaryl)-3-trifluoromethyl-1H-1-phenylpyrazoles (3a-e) (50-85% yields) and 5-alkyl(aryl/heteroaryl)-3-carboxialkyl-1H-1-phenylpyrazoles ...
Determinação multirresíduo de agrotóxicos em berinjela empregando método QuEChERS e UHPLC-MS/MS
(Universidade Federal de Santa Maria, 2022-09-05)
The intensive use of pesticides in agriculture, especially herbicides, insecticides and
fungicides, aims to control pests and diseases in order to increase production. On the
other hand, consumers of these products can ...
Nanopartículas de copolímero em bloco de maltoheptaose-b-polimetilmetacrilato contendo ftalocianina de cloro-alumínio para o uso em terapia fotodinâmica
(Universidade Federal de Santa Maria, 2022-08-09)
New nanocarriers have been contributing to the development of so-called third-generation
photosensitizers for use in photodynamic therapy (PDT). Chloro-aluminum phthalocyanine
(ClAlPc) is a promising second-generation ...
Determinação de resíduos de agrotóxicos em manga empregando método QuEChERS e UHPLC-MS/MS
(Universidade Federal de Santa Maria, 2022-03-16)
Pesticides are applied from the development of the plant to its production, transport and storage. When not applied correctly, these chemicals can cause harm to human health and the environment. Thus, this work aimed to ...
Desenvolvimento de sistema para piroidrólise para o preparo de papelão hidráulico visando a determinação de halogênios
(Universidade Federal de Santa Maria, 2014-08-14)
A pyrohydrolysis system was developed for sample preparation for halogen
determination in hydraulic cardboard. These materials are used for sealings,
mainly engines and nuclear reactors. Because of the contact of the ...
5-trialometil-4,5-diidro-1h-1-(carbonilpiridil)pirazóis: síntese e atividade biológica frente ao Mycobacterium tuberculosis
(Universidade Federal de Santa Maria, 2008-08-06)
This work describes the synthesis of series of 5-hydroxy-3-[alkyl(aryl/heteroaryl)]-5-trifluoro[chloro]methyl-4,5-dihydro-1H-1(carbonylpyridyl)pyrazoles, obtained from the
reactions of 1,1,1-trihalo-4-[alkyl(aryl/hetero ...
Validação de procedimento analítico empregando SPE e GC-ECD para determinação de pesticidas organoclorados em água e avaliação da permeabilidade destes nos dialisadores utilizados em hemodiálise
(Universidade Federal de Santa Maria, 2004-08-27)
The dialysis of the blood, within which the most applied modality is the haemodialysis, is a method thoroughly used for the treatment of the renal inadequacy. With this treatment, toxic substances accumulated in the patient´s ...
Desenvolvimento e validação de método multirresidual para determinação de pesticidas em café verde utilizando GC-MS (NCI-SIM)
(Universidade Federal de Santa Maria, 2012-01-16)
In this study, was developed and validated a multi-residue method for the
determination of 40 pesticides in green coffee beans. To obtain a very homogeneous
sample, the coffee beans were first milled, followed by a slurry ...