Search
Now showing items 31-40 of 88
Síntese de heterociclos via reações de ciclocondensação de a-etiloxalil e -pirazolil(alquil) b-dimetilaminoenonas com1,2- ou 1,3-Dinucleófilos
(Universidade Federal de Santa Maria, 2009-03-06)
Chemoselective synthesis of ethyl 4-pirimidinecarboxylates and/or ethyl 5-pirimidineoxalates via cyclocondensation reaction of b-dimethylaminoenones [R1C(=O)C(=CNMe2)C(=O)CO2Et, where R1 = Ph, 4-MeC6H4, 4-MeOC6H4, ...
β-Alcoxivinil halometil cetonas: síntese e aplicação na obtenção de haloaril enaminonas, Bis-haloarilenaminonas e 5-diclorometil-3-metil-1H-pirazóis.
(Universidade Federal de Santa Maria, 2005-09-12)
The synthesis of a series of β-enamines compounds
[R2C(O)CH=C(R1)NR3R4, where R2 = CF3, CCl3, CHCl2; R3/R4 = H/Ph, H/4-F-C6H4, H/CH2Ph, H/CH2CH2OH, Me/Ph, Me/n-Bu, Et/ Et, -(CH2)4-, Me/Me] from the reaction of β-alkoxyvinyl ...
Determinação de cádmio, cobre e chumbo por F AAS e GF AAS em plantas medicinais empregando amostragem direta de sólidos
(Universidade Federal de Santa Maria, 2005-07-29)
The main objective of this study was to use alternative systems for the analysis of solids by graphite furnace atomic absorption spectrometry (DSS-GF AAS) and with flame (SS-F AAS) for cadmium, copper and lead in determination ...
Estudo fitoquímico da raiz da espécie Melochia chamaedrys St. Hil
(Universidade Federal de Santa Maria, 2005-11-04)
Melochia chamaedrys St.Hil. is a plant that is locally known as douradinha , it is found in South America, more exactly in the south of Brazil, Argentina, and Uruguay. In the state of Rio Grande do Sul , the species M. ...
Síntese de 2-alquinil telurofenos via reação de sonogashira entre 2-halotelurofeno e 1-alcinos
(Universidade Federal de Santa Maria, 2006-05-29)
We present herein our results of the palladium-catalyzed cross-coupling of 2-halotellurophenes with several terminal alkynes to give acetylenic tellurophene
derivatives in excellent yields. Our initial efforts were devoted ...
Antimicrobial ciprofloxacina em efluente hospitalar: exposição ambiental, avaliação de risco e degradação através de processos avançados de oxidação
(Universidade Federal de Santa Maria, 2006-09-01)
In the present study, the presence of the antimicrobial ciprofloxacin (CIP) in effluent from the first-aid clinic of the University Hospital of Santa Maria (PA-HUSM) and its degradation by advanced oxidation processes ...
Estudo de métodos empregando extração em fase sólida e análise por HPLC-DAD e GC-ECD para a determinação de resíduos de pesticidas em águas e da degradação a campo
(Universidade Federal de Santa Maria, 2007-02-26)
The culture of irrigated rice generates a great impact to the environment, both in the amount and the quality of waters. In this study, a methodology was developed and validated for the determination, in waters, of residues ...
Síntese, propriedades e investigação estrutural de 1,3-diariltriazenos e complexos com Ni(II), Pd(II), Pt(II) e Hg(II)
(Universidade Federal de Santa Maria, 2006-08-04)
Although transition metal complexes with nitrogen coordination spheres involving monocatenated 1,3-diarylsubstituted triazenido ligands (ArNNNAr)−, have been investigated in the last decades, the structure of such compounds ...
Estudo fitoquímico e atividade biológica de Pavonia distinguenda A.ST.- HILL. et naudin e Dorstenia brasiliensis LAM
(Universidade Federal de Santa Maria, 2007-03-01)
From the aerial parts of Pavonia distinguenda the glycosilated flavonoids, tirosilide and astragalina glycolilated flavonoids were isolated, among free b-sitosterol, lupeol, taraxerol, germanicol and from the roots of ...
Síntese e estudo das interações de 3-(fosfato)- e 3-(fosfonamida)-4,4,4-trifluor-but-1-il-carbamatos de etila com a enzima acetilcolinesterase e síntese de 3-carboxietil- e 3-pirimidin-2-il-2-oxo-6-trifluormetil-[1,2,3]oxatiazinanas
(Universidade Federal de Santa Maria, 2007-03-01)
A series of [3-(phosphate)-4,4,4-trifluoro-but-1-yl]-carbamic acid ethyl ester and [3-(phosphonamide)-4,4,4-trifluoro-but-1-yl]-carbamic acid ethyl ester obtained from the reaction of g-amino alcohols (4,4,4-trifluoro-3- ...