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Obtenção quimiosseletiva de trialometil-β-dicetonas via reações de acilação de acetais
(Universidade Federal de Santa Maria, 2009-02-27)
This work presents an Acylation Method of Acetals applied to the quimioseletive obtention of trifluormethyl-β-diketones, incluing acetals derived from not symmetrical ketones and functionalized substituents. Five known ...
5-trialometil-4,5-diidro-1h-1-(carbonilpiridil)pirazóis: síntese e atividade biológica frente ao Mycobacterium tuberculosis
(Universidade Federal de Santa Maria, 2008-08-06)
This work describes the synthesis of series of 5-hydroxy-3-[alkyl(aryl/heteroaryl)]-5-trifluoro[chloro]methyl-4,5-dihydro-1H-1(carbonylpyridyl)pyrazoles, obtained from the
reactions of 1,1,1-trihalo-4-[alkyl(aryl/hetero ...
Validação de procedimento analítico empregando SPE e GC-ECD para determinação de pesticidas organoclorados em água e avaliação da permeabilidade destes nos dialisadores utilizados em hemodiálise
(Universidade Federal de Santa Maria, 2004-08-27)
The dialysis of the blood, within which the most applied modality is the haemodialysis, is a method thoroughly used for the treatment of the renal inadequacy. With this treatment, toxic substances accumulated in the patient´s ...
Decomposição de coque, resíduo de vácuo e petróleo extrapesado por piroidrólise para a determinação de cloro
(Universidade Federal de Santa Maria, 2007-10-26)
In this work, a method for chlorine determination in petroleum coke, vacuum and atmospheric residues and heavy petroleum was developed. The pyrohydrolysis sample decomposition method was used, which consists of sample ...
Síntese, estrutura cristalina e molecular de complexos nos sistemas 1,3-bis(p-azofenil)triazenido e 3-(2-flúorofenil)-1-(4-nitrofenil)triazenido/Pd(II)
(Universidade Federal de Santa Maria, 2002-08-05)
The reaction between palladium chloride and 1,3-bis(pazophenyl)triazenido/pyridine yields the complex trans-bis[1,3-bis(pazophenyl)triazenido]-bis(pyridine)palladium(II), complex (a), which
crystallizes in the triclinic ...
Ferro-processos aplicados à degradação de efluente da produção de trifluralina
(Universidade Federal de Santa Maria, 2002-08-02)
In this work, comparative studies about the performance of iron-processes were
carried out in the pre-treatment of effluent streams samples (under high
concentration) from the trifluralin herbicide production (amination ...
Síntese e análise estrutural de compostos supramoleculares de Cd(II) com o ligante 4,6-dimetilpirimidina-2-tiona
(Universidade Federal de Santa Maria, 2004-03)
This dissertation describes the synthesis and analysis of the supramolecular
compounds α- and β-[Cd(DMPYMT-S)2]n, DMPYMT-S = 4,6-dimethylpyrimidine-2-
thione.
The reaction product of cadmium acetate dihydrate with ...
Estudo da interação entre silício e alumínio extraídos do vidro na presença de soluções para nutrição parenteral
(Universidade Federal de Santa Maria, 2003-08)
Silicon is a non-metal essential to the living organisms due to its role
in the tissues and bones. The most important biological forms of silicon are
the amorphous silica and the monomeric silicic acid. Only the ...
Síntese de Tio- e Selenoacrilonitrilas
(Universidade Federal de Santa Maria, 2002-08-26)
In this work three new methodologies were developed, two for the addition of
HX to chalcogenoacetylenes 3 (Methods B and C) and the third on the synthesis of
chalcogenacrylonitriles 2 (Method A). [...]
Combustão iniciada por microondas e determinação em linha de cádmio e chumbo em plantas por espectrometria de absorção atômica com tubo aquecido na chama
(Universidade Federal de Santa Maria, 2007-02-07)
In this work a new procedure is proposed by solid sampling flame furnace atomic absorption spectrometry after microwave induced combustion (MIC-FFAAS). The procedure was applied for the determination of cadmium and lead ...