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Reações de 1,1,1-tricloro-4-metoxi-3-penten-2-ona com hidrazinas monosubstituídas
(Universidade Federal de Santa Maria, 2005-02-18)
The 1,1,1-trichloro-4-methoxy-3-penten-2-ona (CCl3COCH=CHOMe) reaction with hydrazines series (RNHNH2, where R = H, Me, tert-Bu, Ph, Ph(F)5, Ph-4-NO2, CO2Me e CONH2) yield to the pyrazoles N-substituted and derivatives ...
Reatores de discos rotativos e tubular helicoidal na degradação fotocatalítica de diclofenaco e carga orgânica de efluente hospitalar
(Universidade Federal de Santa Maria, 2009-07-28)
In this study, the advanced oxidation process heterogeneous photocatalysis were used for the degradation of diclofenac and decrease of the organic load in the effluent from the emergency sector (PA) of the University ...
Arranjos supramoleculares de triazenidos complexos de Ag(I) através de ligações de hidrogênio
(Universidade Federal de Santa Maria, 2008-08-14)
In this work we synthesized and determinates the crystaline/molecular structure of thre Ag(I) complexes, all of them use monocatenated triazenide ligands previously desprotonated. The complex [Ag(C6H4FNNNC6H4NO2)(C5H5N)]2 ...
Síntese, caracterização e cristaloquímica de complexos da cobre(I) e mercúrio(II) com ligantes triazenidos
(Universidade Federal de Santa Maria, 2005-07-20)
The reaction between mercury(II) acetate and 1-(3-nitrophenyl)-3-(2-fluorophenyl)triazene in a tetrahydrofuran/methanol mixture in the presence of
2,2′-bipiridylamine yields the complex [Hg(FC6H4NNNC6H4NO2)2] (1). (1) ...
Síntese de 2-(1h-pirazol-1-il)-5-(1h-pirazol-1-il-1-carbonil) piridinas
(Universidade Federal de Santa Maria, 2008-02-20)
This work describes the synthesis of a new series of 2-[3-alkyl(aryl/heteroaryl)-5-trihalomethyl-5-hydroxy-4,5-dihydro-1H-pyrazol-1-il]-5-[3-alkyl(aryl/heteroaryl)-5-trihalomethyl-5-hydroxy-4,5-dihydro-1H-pyrazol-1-il-1- ...
Síntese de 1,7-fenantrolinas e 7-aminoquinolinas trifluormetil substituídas
(Universidade Federal de Santa Maria, 2010-02-26)
This work, at first, describes the synthesis and characterization of new series of (Z,Z)-N,N -bis(oxotrifluoroalkenyl)-1,3-phenylenediamines by the addition/elimination reaction of β-alkoxyvinyl trifluoromethyl ketones ...
Síntese e estereoquímica de isoxazóis espiro-tetracíclicos trifluormetil substituídos
(Universidade Federal de Santa Maria, 2017-02-23)
The present dissertation initially describes methodologies for the synthesis of five 3-(trifluoromethyl)-3,3a-dihydrospiro[chromeno[4,3-c]isoxazole-4,1'-cycloalkan]-3-ols (7) in 65 – 84 % yields, where the spirocarbocyclic ...
Determinação de elementos do grupo da platina em carvão com alto teor de cinzas por ICP-MS
(Universidade Federal de Santa Maria, 2017-06-03)
In this work a method for the digestion of high ash content coal (>30%) using a high
pressure asher (HPA) system for further determination of platinum group elements
(PGEs) by inductively coupled plasma mass spectrometry ...
Avaliação do comportamento de espécies de mercúrio em peixes após diferentes métodos de cocção
(Universidade Federal de Santa Maria, 2011-03-22)
Most of studies evaluating Hg in fish have been developed using fresh fish and
the few studies involving the assessment of Hg in fish after cooking process, involve
only the determination of total Hg and no clear conclusions ...
Avaliação de métodos de preparo de amostras para a determinação de cloro em temperos
(Universidade Federal de Santa Maria, 2012-05-24)
In this study, sample preparation methods were evaluated for the
determination of chlorine by ion chromatography (IC) in spice samples. The
microwave-induced combustion method (MIC) was tested using certified ...