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Determinação simultânea de ácido clavulânico e amoxicilina em formulações farmacêuticas utilizando técnicas de reflexão no infravermelho médio e métodos de regressão multivariados
(Universidade Federal de Santa Maria, 2009-08-14)
Clavulanic acid (AC) and amoxicillin (AMO) drugs are used in association and they are commercialized in Brazil as antibiotic agent. The simultaneous determination of
these drugs is, usually, carried out by high performance ...
Reatores de discos rotativos e tubular helicoidal na degradação fotocatalítica de diclofenaco e carga orgânica de efluente hospitalar
(Universidade Federal de Santa Maria, 2009-07-28)
In this study, the advanced oxidation process heterogeneous photocatalysis were used for the degradation of diclofenac and decrease of the organic load in the effluent from the emergency sector (PA) of the University ...
Síntese e caracterização de β-dicetonas 4,4,4-tricloro-1-aril-1,3-butanodionas e seus respectivos β-dicetonatos de cobre e ferro
(Universidade Federal de Santa Maria, 2009-07-31)
The present dissertation describe, initially, the synthesis of a new series of 4,4,4-trichloro-1-aryl-1,3-butanediones (3a-l) [Cl3CCOCHRCOR1], where R=H, CH3 and R1 = Ph, 4-CH3Ph, 3-OCH3Ph, 4-OCH3Ph, 4-FPh, 4-ClPh, 4-
BrPh, ...
Comparação entre os métodos de extração quechers e miniluke modificados na extração de resíduos de pesticidas piretróides em tomate empregando GC×GC-μECD
(Universidade Federal de Santa Maria, 2009-08-29)
In this study, two methods frequently used in the extraction of residues of pesticides in fruits and vegetables, the QuEChERS method and the mini-Luke
method, were compared in order to optimize and validate these methods ...
Desenvolvimento de equipamento de eletroforese capilar com detecção por condutividade sem contato para a separação de íons inorgânicos
(Universidade Federal de Santa Maria, 2009-03-16)
This work describes the development and evaluation of a home-made capillary electrophoresis (CE) system based on the capacitively coupled contactless conductivity
detection (C4D) for the application in capillary ...
Desenvolvimento de métodos eletroforéticos e cromatográficos para a determinação de benzodiazepínicos como adulterantes em formulações fitoterápicas para emagrecimento
(Universidade Federal de Santa Maria, 2009-07-03)
The adulteration of phytotherapic formulations has been increasing considerably in the recent years in several countries, by the fact that there is not an
established efficient monitoring for the control of the manipulation ...
Especiação de mercúrio em cogumelos por LC-CVG-ICP-MS: avaliação de procedimentos de extração
(Universidade Federal de Santa Maria, 2009-07-31)
In this work, different sample preparation procedures for determining inorganic (in Hg2+ form) and organic mercury (in methylmercury form CH3Hg+) in edible mushrooms were evaluated. Conventional, microwave (MW) and ...
Síntese e caracterização de novos compostos de difenilfosfinatos de chumbo(II) e mercúrio(I) e (II)
(Universidade Federal de Santa Maria, 2009-08-17)
In this work, nine new compounds of lead(II) and mercury(I) and (II)diphenylphosphinates were synthesized, among them four are lead(II) compounds with diphenylphosphinates, hydroxo and water ligands, obtained in reactions ...
Síntese e análise estrutural de complexos de Urânio e Vanádio com ligantes derivados da piridoxina
(Universidade Federal de Santa Maria, 2009-12-11)
Uranyl and vanadyl complexes with ligands with oxygen and nitrogen donors atoms have been extensively reviewed and aroused remarkable interest on account their high
stability but, a few complexes of piridoxine derived ...
Estudo da interação entre alumínio e os constituintes de formulações de eritropoetina empregando HPLC e AAS
(Universidade Federal de Santa Maria, 2009-03-05)
Erythropoietin (EPO) is a glycoprotein which stimulates the erythropoiesis (production of hemaceas) and is clinically used for the treatment of renal anemia. EPO formulations present usually elevated contamination by ...