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Avaliação de métodos de preparo de amostras para posterior determinação de contaminantes inorgânicos em cápsulas de uso farmacêutico
(Universidade Federal de Santa Maria, 2014)
In this work, sample preparation methods were proposed, microwave-induced combustion (MIC) and microwave-assisted wet digestion (MAWD), for further Br, Cl, Cr, Cu, I and Mn determination in pharmaceutical capsules. For Cl, ...
Desenvolvimento de métodos de preparo de amostras para posterior determinação de As, Cd e Pb em carne e produtos cárneos
(Universidade Federal de Santa Maria, 2012-12-05)
Sample preparation methods, such as microwave-assisted wet digestion, dry ashing, wet digestion in open system and tetramethylammonium hydroxide (TMAH) solubilization were evaluated for subsequent As, Cd and Pb determination ...
Determinação de elementos traço em solo por ICP-MS após volatilização empregando combustão iniciada por micro-ondas
(Universidade Federal de Santa Maria, 2011-03-22)
In this work the microwave-induced combustion (MIC) method was proposed for the decomposition of soil samples and subsequent determination of As, Bi, Cd, Hg, Pb and Se by inductively coupled plasma mass spectrometry (ICP-MS). ...
Método multirresíduo para determinação de micotoxinas em vinho por UPLC-MS/MS
(Universidade Federal de Santa Maria, 2013-01-08)
A fast multimethod using liquid chromatography tandem mass spectrometry (UPLC-MS/MS) was implemented and optimized to yield a complete determination of 36 mycotoxins in wine samples. Extraction was performed with acetonitrile, ...
Avaliação de métodos de decomposição de chocolate e determinação de metais por ICP-OES e ICP-MS
(Universidade Federal de Santa Maria, 2014-02-13)
In this work, was evaluated the main methods of sample preparation reported in the literature for decomposition of chocolate and, in addition, was proposed the decomposition by microwave induced combustion (MIC) for further ...
Determinação de enxofre em amostras de grafite flexível por ICP OES utilizando piroidrólise como preparo de amostra
(Universidade Federal de Santa Maria, 2013-07-16)
The flexible graphite is a material produced from the intercalation, exfoliation
and compression of graphite. Due to its low porosity, high chemical and thermal
resistance, the flexible graphite is used in many different ...
Desenvolvimento de metodologia para a determinação de contaminantes inorgânicos em polímeros por LA-ICP-MS
(Universidade Federal de Santa Maria, 2016-02-23)
In the present work a new calibration strategy was evaluated for further determination of As, Ba, Cd, Cr, Pb, Sr and Zn in food packaging by laser ablation and inductively coupled plasma mass spectrometry (LA-ICP-MS). The ...
Determinação de halogênios em mel após decomposição com peróxido de hidrogênio usando sistema de alta pressão
(Universidade Federal de Santa Maria, 2016-02-12)
In this work the sample preparation method for honey decomposition using H2O2 in alkaline medium at high pressure system for further determination of F, Cl, Br and I was evaluated. In this way, some parameters such as ...
Determinação de Ca, K, Mg e Na em petróleo utilizando amostragem direta e espectrometria de absorção atômica com forno de grafite
(Universidade Federal de Santa Maria, 2015-07-27)
Crude oil is a complex matrix and with variable chemical composition, and the determination of trace elements in this sample is not an easy task. The presence of some metals can result in problems during transportation and ...
Aplicação de ultrassom para remoção de enxofre e de nitrogênio do óleo diesel: avaliação de parâmetros do processo e determinação de enxofre e de nitrogênio por técnicas espectrométricas e cromatográficas
(Universidade Federal de Santa Maria, 2011-09-29)
In the present work, the ultrasound assisted oxidation of sulfur and nitrogen compounds present in diesel fuel was investigated. The oxidized compounds are more polar than their original forms and can be removed from oil ...