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Determinação de As, Bi, Sb, Se, Sn e Te por injeção em fluxo com geração de hidretos acoplada a espectrometria de massa com plasma indutivamente acoplado
(Universidade Federal de Santa Maria, 2010-07-23)
In this work it is proposed the development of flow injection systems for hydride generation coupled to inductively coupled plasma mass spectrometry (FI-HG-ICPMS)
for determination of trace elements (As, Bi, Sb, Se, Sn and ...
Determinação de cloridrato de propranolol em medicamentos por espectroscopia no infravermelho com calibração multivariada (PLS)
(Universidade Federal de Santa Maria, 2005-07-21)
In this work calibration multivariate models were developed with the use of the technique of partial least scores (PLS) for the dosage of tablets of propranolol hydrochloride using infrared spectroscopy. Samples were ground ...
Análise de dados de RMN, deslocamentos químicos e constantes de acoplamento do sistema de hidrogênios ABX em 3,5-diaril-4,5-diidro-1H-pirazóis
(Universidade Federal de Santa Maria, 2012-09-10)
This dissertation first describes the collection of literature data among the years 2005 to 2011 for the subsequent data analysis of 1H NMR chemical shifts and coupling constants and 2JHH 3JHH with emphasis on the synthesis ...
Sintese, análise estrutural e supramolecular de complexos triazenido de Ag(I), Cd(II) E Zn(II)
(Universidade Federal de Santa Maria, 2011-05-23)
In this work was synthesized and determined the crystal and molecular
structure of two silver triazenide complexes, two cadmium triazenide complexes
and a zinc triazenide complex. The complexes
{Ag[C12H9N2NNNC6H4(NO2)](C5H5N)}2 ...
Determinação de cádmio, cobre e chumbo em catalisadores por espectrometria de absorção atômica com forno de grafite e amostragem direta de sólidos
(Universidade Federal de Santa Maria, 2006-07-26)
Trace impurities of Cd, Cu and Pb were determined in alumina-based catalysts using direct solid sampling graphite furnace atomic absorption spectrometry (DSS-GF AAS). The analyzed catalysts are widely used in petrochemical ...
Determinação de elementos traço em solo por ICP-MS após volatilização empregando combustão iniciada por micro-ondas
(Universidade Federal de Santa Maria, 2011-03-22)
In this work the microwave-induced combustion (MIC) method was proposed for the decomposition of soil samples and subsequent determination of As, Bi, Cd, Hg, Pb and Se by inductively coupled plasma mass spectrometry (ICP-MS). ...
Reações de 2-alcóxi-5-trifluoracetil-3,4-diidro-2H-piranos com etilaminas substituídas e arilaminas
(Universidade Federal de Santa Maria, 2011-02-25)
This work presents the synthesis of two novel series of 1-alkyl(aryl)-2-amino-
5-trifluoroacetyl-1,2,3,4-tetrahydropyridine (6, 8), obtained from the reaction of 2-
alkoxy-5-trifluoroacetyl-3,4-dihydro-2H-pyrans (alkoxy = ...
Síntese de 1-aril-4-[(dimetilamino)metileno] pirrolidino-2,3,5-trionas utilizando irradiação de micro-ondas
(Universidade Federal de Santa Maria, 2011-02-24)
The synthesis of a series of 1-aryl-4-[(dimethylamino)methylene] pyrrolidine-
2,3,5-trione from the cyclocondensation reaction between b-enaminodiketone
[Cl3C(O)C(=CHNMe2)C(O)CO2Et] and aniline derivatives [R = Ph, 3-Me-C6H4, ...
Síntese de β-Calcogenoaminas quirais via abertura regiosseletiva de Aziridinas em Líquidos Iônicos.
(Universidade Federal de Santa Maria, 2011-07-29)
The present work report the synthesis of β-chalcogen amino compounds derived from L-aminoacids. The desired products were obtained in a short reaction time, with high yields using a simple and environmentally friendly ...
Nh-pirazóis e isoxazóis: síntese mecanicamente ativada por grinding
(Universidade Federal de Santa Maria, 2010-07-30)
The synthesis of twelve NH-pyrazoles from the cyclocondensation reaction of β-dimethylaminovinylketones ([R1C(O)C(R2)=CHN(Me)2], where R1 = Me, C6H5, 3-
MeO-C6H4, 4-Me-C6H4, 4-MeO-C6H4, 4-F-C6H4, 4-Cl-C6H4, 4-Br-C6H4, ...