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Itens para a visualização no momento 11-20 of 1417
Determinação simultânea de ácido clavulânico e amoxicilina em formulações farmacêuticas utilizando técnicas de reflexão no infravermelho médio e métodos de regressão multivariados
(Universidade Federal de Santa Maria, 2009-08-14)
Clavulanic acid (AC) and amoxicillin (AMO) drugs are used in association and they are commercialized in Brazil as antibiotic agent. The simultaneous determination of
these drugs is, usually, carried out by high performance ...
Reatores de discos rotativos e tubular helicoidal na degradação fotocatalítica de diclofenaco e carga orgânica de efluente hospitalar
(Universidade Federal de Santa Maria, 2009-07-28)
In this study, the advanced oxidation process heterogeneous photocatalysis were used for the degradation of diclofenac and decrease of the organic load in the effluent from the emergency sector (PA) of the University ...
Síntese e caracterização de β-dicetonas 4,4,4-tricloro-1-aril-1,3-butanodionas e seus respectivos β-dicetonatos de cobre e ferro
(Universidade Federal de Santa Maria, 2009-07-31)
The present dissertation describe, initially, the synthesis of a new series of 4,4,4-trichloro-1-aryl-1,3-butanediones (3a-l) [Cl3CCOCHRCOR1], where R=H, CH3 and R1 = Ph, 4-CH3Ph, 3-OCH3Ph, 4-OCH3Ph, 4-FPh, 4-ClPh, 4-
BrPh, ...
Determinação de espécies de antimônio em antimoniato de meglumina
(Universidade Federal de Santa Maria, 2008-08-04)
In this study different methods for speciation of Sb(III) and Sb(V) in meglumine
antimoniate (NMG) were evaluated. Liquid chromatography (LC) combined or not
with hydride generation (HG) was investigated for separation of ...
Quantificação do alumínio administrado e excretado em recém-nascidos pré-termo em uma unidade de terapia intensiva neonatal
(Universidade Federal de Santa Maria, 2008-10-15)
Al is a ubiquitous element on the earth crust and is considered a non-essential
element for humans since it is not involved in any biochemical process. Aluminum
may act as a toxic species when it is introduced directly ...
Arranjos supramoleculares de triazenidos complexos de Ag(I) através de ligações de hidrogênio
(Universidade Federal de Santa Maria, 2008-08-14)
In this work we synthesized and determinates the crystaline/molecular structure of thre Ag(I) complexes, all of them use monocatenated triazenide ligands previously desprotonated. The complex [Ag(C6H4FNNNC6H4NO2)(C5H5N)]2 ...
Desenvolvimento e validação de método multirresíduo, empregando GC-ECD E GC-MS, para a investigação de pesticidas em morango, maçã e uva
(Universidade Federal de Santa Maria, 2005-03-03)
Pesticides use is still the main strategy used in the field for the combat and the prevention of agricultural plagues, guaranteeing enough food and of quality for the population. In the culture of fruits, especially in ...
Avaliação da associação molecular de complexos metálicos com ligante triazenido 1-óxido
(Universidade Federal de Santa Maria, 2008-06-16)
In this dissertation were synthetized six compounds, of the which one is free ligand 1- phenyl-3-(4-nitrophenyl) triazene 1-oxide (1) and five are triazenido complexes of [Ni(O2NC6H4NNN(O)C6H5)2(C5H5N)2] (2), [Zn(O2NC6H4 ...
Reações de ciclocondensação de cianoacetoidrazida com enonas halometil-substituídas
(Universidade Federal de Santa Maria, 2008-02-22)
The synthesis of thirteen 3-(R1), 4-(R2) and 5-(R3)-substituted 1-cyanoacetyl-5-hydroxy-4,5-dihydro-1H-pyrazoles from the cyclocondensation reaction of 4-alkoxy-3-alken-2-ones [R3C(O)C(R2)=C(R1)(OR), where R3 = CF3,
CCl3, ...
Síntese de trifluormetil-cicloalca[d]-2(1h)-pirimidinonas e tiopirimidinonas
(Universidade Federal de Santa Maria, 2004-07-20)
This work describes the synthesis and identification of a serie of 4-trifluoromethylcycloalca[d]-2-(1H)-(thio)pyrimidinones, from the cyclocondensation reactions of 2-trifluoroacetylmethoxycycloalkenes with urea and ...