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Determinação de espécies de antimônio em antimoniato de meglumina
(Universidade Federal de Santa Maria, 2008-08-04)
In this study different methods for speciation of Sb(III) and Sb(V) in meglumine
antimoniate (NMG) were evaluated. Liquid chromatography (LC) combined or not
with hydride generation (HG) was investigated for separation of ...
Quantificação do alumínio administrado e excretado em recém-nascidos pré-termo em uma unidade de terapia intensiva neonatal
(Universidade Federal de Santa Maria, 2008-10-15)
Al is a ubiquitous element on the earth crust and is considered a non-essential
element for humans since it is not involved in any biochemical process. Aluminum
may act as a toxic species when it is introduced directly ...
Arranjos supramoleculares de triazenidos complexos de Ag(I) através de ligações de hidrogênio
(Universidade Federal de Santa Maria, 2008-08-14)
In this work we synthesized and determinates the crystaline/molecular structure of thre Ag(I) complexes, all of them use monocatenated triazenide ligands previously desprotonated. The complex [Ag(C6H4FNNNC6H4NO2)(C5H5N)]2 ...
Avaliação da associação molecular de complexos metálicos com ligante triazenido 1-óxido
(Universidade Federal de Santa Maria, 2008-06-16)
In this dissertation were synthetized six compounds, of the which one is free ligand 1- phenyl-3-(4-nitrophenyl) triazene 1-oxide (1) and five are triazenido complexes of [Ni(O2NC6H4NNN(O)C6H5)2(C5H5N)2] (2), [Zn(O2NC6H4 ...
Reações de ciclocondensação de cianoacetoidrazida com enonas halometil-substituídas
(Universidade Federal de Santa Maria, 2008-02-22)
The synthesis of thirteen 3-(R1), 4-(R2) and 5-(R3)-substituted 1-cyanoacetyl-5-hydroxy-4,5-dihydro-1H-pyrazoles from the cyclocondensation reaction of 4-alkoxy-3-alken-2-ones [R3C(O)C(R2)=C(R1)(OR), where R3 = CF3,
CCl3, ...
Síntese de 2-(1h-pirazol-1-il)-5-(1h-pirazol-1-il-1-carbonil) piridinas
(Universidade Federal de Santa Maria, 2008-02-20)
This work describes the synthesis of a new series of 2-[3-alkyl(aryl/heteroaryl)-5-trihalomethyl-5-hydroxy-4,5-dihydro-1H-pyrazol-1-il]-5-[3-alkyl(aryl/heteroaryl)-5-trihalomethyl-5-hydroxy-4,5-dihydro-1H-pyrazol-1-il-1- ...
Síntese de 5-hidróxi-3-(1,1-dimetoxietan-2-il)-5-trifluormetil-2-pirazolinas e 3-(1,1-difluoretan-2-il)-1H-pirazóis análogos
(Universidade Federal de Santa Maria, 2008-02-01)
This work describes, at first, the synthesis of 4,6,6-trimethoxy-1,1,1-trifluorohex-3-en-2-one by the acylation reaction of 1,1,3,3-tetramethoxybutane, in 65% yields.
Afterwards, the synthesis of a new series of ...
Variações espaciais de propriedades físicas do remanescente de supernova RCW 103
(Universidade Federal de Santa Maria, 2008-06-19)
Since the observation of the supernova event SN 1987A, observational research on supernova and supernova remnants, including the ones on the optical spectrum,
has been much explored. However, most of these studies have ...
Estudo do ciclo diário da camada limite planetária através da simulação dos grandes turbilhões
(Universidade Federal de Santa Maria, 2008-12-15)
The PBL is the region on the troposphere characterized by existence of turbulence (BUSINGER, 1981). Turbulent flow is that when the fluctuations of the variables that describe the flow are amplified in time and space ...
Modelagem lagrangeana aplicada à dispersão de contaminantes em diferentes condições de estabilidade atmosférica
(Universidade Federal de Santa Maria, 2008-04-25)
In this dissertation, it was estimated contaminants concentration in different stability conditions of the Planetary Boundary Layer. In order to do this, it was used the Lagrangian stochastic model. The experiments by ...