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Produção e caracterização de carvão ativado modificado por sonicação e sua aplicação na adsorção de fármacos
(Universidade Federal de Santa Maria, 2019-02-08)
Water pollution by emerging contaminants such as pharmaceuticals has gained interest in recent
years. These drugs have great potential in generating adverse effects for human and wildlife,
since they are endocrine ...
Formação de ligações carbono-nitrogênio e carbonocalcogênio catalisadas por iodeto de cobre: síntese de 2- (organocalcogenil)-indolizinas
(Universidade Federal de Santa Maria, 2018-02-28)
The copper-catalyzed cyclization of propargylpyridines with diorganyl
dichalcogenides was applied to the synthesis of 2-(organochalcogenyl)-indolizines.
A systematic study of the cyclization system revealed that the ...
Síntese, estrutura e avaliação antimicobacteriana de novos 1- (espiro[croman-2,1’-cicloalcan]-4-il)-1h-1,2,3-triazóis
(Universidade Federal de Santa Maria, 2018-08-03)
This thesis describes the synthesis, structural study and antimycobacterial evaluation of a series of novel
4-(alkyl/aryl)-1-(spiro[chroman-2,1'-cycloalkan]-4-yl)-1H-2,3-triazoles having as substituent aryl = phenyl, ...
Síntese de novos pirróis derivados de aminocumarinas
(Universidade Federal de Santa Maria, 2018-07-19)
In this work, the synthesis of new pyrroles derived from aminocoumarins was
developed. First, the synthesis of pyrroles derived from 4-amino-2H-chromen-2-one
was carried out by the Paal-Knorr and Clauson-Kaas reactions, ...
Síntese e caracterização estrutural de novos compostos organocalcogenoxanos contendo ítrio(III)
(Universidade Federal de Santa Maria, 2017-07-26)
This work describes the synthesis and structural characterization of new organochalcogenoxanes polymer and clusters compounds containing yttrium(III) ion. The synthetized compounds have structure of unidimensional coordination ...
Síntese e caracterização de 1,3,4-oxadiazolil-1,2,4-oxadiazóis derivados de ácidos acrílicos 3-substituídos
(Universidade Federal de Santa Maria, 2017-02-24)
A series of 1,3,4-oxadiazolyl-1,2,4-oxadiazoles was synthesized through a one-pot condensation-cyclization reaction between 3-substituted acrylic acids and 5-aryl-1,2,4-oxadiazolyl-1,2,4-oxadiazoles, and were characterized ...
Autoassociação de amidas aromáticas: abordagem supramolecular e mecanismos de cristalização
(Universidade Federal de Santa Maria, 2017-07-21)
This work presents the use of N-phenylamides as models for the study of self-association and intermolecular interactions. Obtaining the crystal of N-phenyltrifluoroacetamide allowed its diffraction and inclusion in the ...
Síntese e estereoquímica de isoxazóis espiro-tetracíclicos trifluormetil substituídos
(Universidade Federal de Santa Maria, 2017-02-23)
The present dissertation initially describes methodologies for the synthesis of five 3-(trifluoromethyl)-3,3a-dihydrospiro[chromeno[4,3-c]isoxazole-4,1'-cycloalkan]-3-ols (7) in 65 – 84 % yields, where the spirocarbocyclic ...
Síntese de 4-(1-fenil-5-trifluormetil-1h-pirazol-4-il)-1h-1,2,3-triazóis promovida por dialquil biaril fosfinas e catálise metálica
(Universidade Federal de Santa Maria, 2017-08-11)
The present dissertation describes the development of a three-step, one-pot methodology, involving the sequential reactions of Sonogashira cross-coupling, deprotection of terminal alkyne (removal of trimethylsilane group), ...
Caracterização e avaliação da atividade fotodinâmica de tetra-meso-[(piridil)porfirina]platina(II) frente à microorganismos
(Universidade Federal de Santa Maria, 2017-06-30)
This work deals with the synthesis of Tetra-meso-[(3-pyridyl)-chloro-2,2'-bipyridyl-platinum(II)]porphyrin (3-H2TPtPyP) and Tetra-meso-[(4-pyridyl)-chloro-2,2'-bipyridyl-platinum(II)]porphyrin (4-H2TPtPyP), starting from ...