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Decomposição de elastômeros por combustão iniciada por microondas em sistema fechado
(Universidade Federal de Santa Maria, 2006-07-28)
A rapid digestion procedure for further determination of inorganic elements in carbon black-containing elastomers has been developed using sample combustion in closed quartz vessels with oxygen pressure. Microwave radiation ...
Investigação sobre a formação de espécies de arsênio orgânico em soluções de nutrição parenteral
(Universidade Federal de Santa Maria, 2006-06-21)
Parenteral nutrition is the nutrients administration by intravenous mean in patients who cannot consume them for gastrointestinal way. Parenteral Nutrition Solutions are stored in glass and plastic containers, being the ...
Análise estrutural de polímeros bidimensionais de fosfinatos de metais alcalinos e alcalinos terrosos
(Universidade Federal de Santa Maria, 2006-03-03)
In this work, the structures of three alkali and alkali-earth metal complexes of
phenylphosphinate ligands and ethylphosphinate ligands, (4) catena-poli-
[Ba(O2PHPh)2(OH2)], (5) catena-poli-[Na(O2PHPh)] e (6) ...
Antimicrobial ciprofloxacina em efluente hospitalar: exposição ambiental, avaliação de risco e degradação através de processos avançados de oxidação
(Universidade Federal de Santa Maria, 2006-09-01)
In the present study, the presence of the antimicrobial ciprofloxacin (CIP) in effluent from the first-aid clinic of the University Hospital of Santa Maria (PA-HUSM) and its degradation by advanced oxidation processes ...
Determinação de espécies de arsênio, antimônio e chumbo em antimoniato de meglumina por espectrometria de absorção atômica após extração em fase sólida
(Universidade Federal de Santa Maria, 2006-12-01)
In this study, two flow systems with a solid phase extraction were developed for the determination of Sb(III), Pb(II) As(V) and total As by atomic absorption spectrometry in sample of meglumine antimonate, which is the ...
Pirazolo[1,5-a]pirimidinas: síntese e bromação
(Universidade Federal de Santa Maria, 2006-01-27)
The synthesis of a series of 2-methyl-7-trichloromethylpyrazolo[1,5-a]pyrimidines from the cyclocondensation reaction of 3-amino-5-methylpyrazole with 1,1,1-trichloro-4- alkoxyalk-3-en-2-ones [CCl3C(O)CH=C(R1)OR where R1 ...
Síntese e análise estrutural de complexos de urânio(VI) com hidrazonas, semicarbazonas e ligantes relacionados
(Universidade Federal de Santa Maria, 2006-10-02)
Uranyl complexes with ligands with oxygen and nitrogen donors have been extensively reviewed and they have aroused interest on account of their high stability, usefulness in selective chemical separations and their formation ...
Síntese de 3H-pirido[2,3-b][1,4]diazepinos trifluormetil substituídos e diazepinonas análogas
(Universidade Federal de Santa Maria, 2006-12-19)
The present research describes new synthetic methodologies for the synthesis of new series of 2-aryl(heteroaryl)-4-trifluoro-4,5-dihydro-3Hpyrido[2,3-b][1,4]diazepin-4-ols and 2-aryl(heteroaryl)-3H-pyrido[2,3-b][1,4]diaz ...
Investigação de complexos binucleares de K+ E CU(II) com ligantes 1,3-diariltriazenidos simétricos
(Universidade Federal de Santa Maria, 2006-12-15)
At work present it synthesized and determined itself the molecular structure of a copper complex (II) and another of potassium in which both involve triazenides ligands
monocatenados previously deprotonated. The reaction ...
Síntese e caracterização estrutural de pirazolinil-tolil-sulfonas trialometil substituídas de interesse antimicrobiano
(Universidade Federal de Santa Maria, 2006-02-02)
The present research describes the use of b-alcoxyvynil
trihalomethyl ketones [CX3C(O)CR2CR1R, where X= Cl, F; R= OMe, OEt; R1: H, Me, Ph, 4-MePh, 4-MeOPh, 4-BrPh, 4-ClPh, 4-FPh; R2= H, Ph] in the regiospecific synthesis ...