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Síntese e estereoquímica de isoxazóis espiro-tetracíclicos trifluormetil substituídos
(Universidade Federal de Santa Maria, 2017-02-23)
The present dissertation initially describes methodologies for the synthesis of five 3-(trifluoromethyl)-3,3a-dihydrospiro[chromeno[4,3-c]isoxazole-4,1'-cycloalkan]-3-ols (7) in 65 – 84 % yields, where the spirocarbocyclic ...
Determinação de elementos do grupo da platina em carvão com alto teor de cinzas por ICP-MS
(Universidade Federal de Santa Maria, 2017-06-03)
In this work a method for the digestion of high ash content coal (>30%) using a high
pressure asher (HPA) system for further determination of platinum group elements
(PGEs) by inductively coupled plasma mass spectrometry ...
Síntese de pirrolocumarinas via nitroestirenos e de novos selenetos derivados da cumarina
(Universidade Federal de Santa Maria, 2017-03-08)
This work describes the synthesis of pyrrolo[3,2-c]coumarins from 4-aminophenylcoumarins and nitrostyrenes (17 examples), which were obtained in yelds between 6 and 76 % in a reaction catalised by PTSA.H2O and under ...
Decomposição assistida por radiação micro-ondas e ultravioleta de resíduos de equipamentos elétricos e eletrônicos para determinação de Br, Cd, Cr, Hg, Pb e Sb
(Universidade Federal de Santa Maria, 2017-03-09)
In this work, a method for ultraviolet and microwave-assisted wet digestion (MAWD-UV) was developed for digestion of waste electrical and electronic equipment (WEEE) for further determination of Br, Cd, Cr, Hg, Pb and Sb ...
Desenvolvimento de método de preparo de amostras baseado no efeito Maxwell-Wagner e determinação de elementos terras raras por técnicas espectrométricas
(Universidade Federal de Santa Maria, 2017-06-03)
A new method for analytical applications based on Maxwell-Wagner effect with to use of microwave radiation in closed system is proposed. Considering the interaction of carbonaceous materials with an oscillating electromagnetic ...
Decomposição de amostras de alimentos empregando ácido nítrico diluído e pressurização com diferentes gases em sistema de câmara única de reação assistida por radiação micro-ondas
(Universidade Federal de Santa Maria, 2017-03-23)
In the present work the use of a microwave-assisted wet digestion using a single reaction chamber system (MAD-SRC) at high pressure and temperature was evaluated for digesting food samples. It was evaluated the use of ...