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Aplicação de 5-bromo-1,1,1-trifluor-4-metoxipent-3-en-2-ona na síntese de pirróis, pirazóis, pirimidinas e 1,2,3-triazóis
(Universidade Federal de Santa Maria, 2015-10-30)
This thesis reports the synthesis of various series of trifluoromethyl substituted nitrogenated heterocycles, such as pyrroles, pyrazoles, pyrimidines and 1,2,3-triazoles, exploiting the synthetic versatility of ...
Síntese de copolímeros em bloco por reações one-pot com processos RAFT e ROP simultâneos
(Universidade Federal de Santa Maria, 2016-02-04)
The present work describes a methodology of controlled synthesis of block copolymers by one-pot reactions involving simultaneous RAFT and ROP processes mediated by a bifunctional compound which acts as a chain transfer ...
HPAs em águas superficiais e efluente hospitalar: degradação por PAOs e desenvolvimento de métodos para determinação e identificação de subprodutos
(Universidade Federal de Santa Maria, 2016-02-26)
In this study, was optimization an analytical method for identification and quantification method of Polycyclic Aromatic Hydrocarbons (PAHs) in surface water and hospital effluent samples. High Performance Liquid Chromatography ...
Determinação de POPs e agrotóxicos em leite materno empregando cromatografia a gás acoplada à espectrometria de massas com ionização química negativa (GC-NCI-MS)
(Universidade Federal de Santa Maria, 2016-03-31)
The Stockholm Convention was the first global attitude trying to preserve human health and the environment of the indiscriminate use of persistent organic pollutants (POPs), especially pesticides, which are characterized ...
Síntese e avaliação da atividade antioxidante de calcogenilazidas e calcogeniltriazóis
(Universidade Federal de Santa Maria, 2016-03-24)
In this work, we developed a synthetic route for obtaining β-aryl-chalcogenoazide and β-aryl-chalcogenotriazole (S, Se and Te) derived from L-amino acids (L-phenylalanine, L-valine and L-leucine). We obtained a compounds ...
Síntese e bioatividade de sistemas pirazolil-piridínicos poli-heterocíclicos trialometil substituídos
(Universidade Federal de Santa Maria, 2015-03-02)
This thesis describes the studies carried out using the reagent 6-
hydrazinonicotinic hydrazide for the synthesis of new trihalomethylated pyrazolylpyridine
systems using the 4-alkoxy-4-alkyl(aryl/heteroaryl-1,1,1-trihal ...
Síntese de novas azinas trifluormetil substituídas e derivados a partir de reações de heterociclização de trifluoracetil enol éteres com diamino arenos
(Universidade Federal de Santa Maria, 2013-12-13)
The present research describes the study of synthetic strategies for obtaining of polyheterocyclic systems trifluoromethyl substituted from simple precursors: 4-alkoxy-1,1,1-trifluoroalk-3-en-2-ones (1), of formula ...
Síntese de heterociclos: 2-alquil/arilcalcogeno-n-(4-aril-1,3-tiazol-2-il)acetamidas e (s)-n-(1-(3-aril-1,2,4-oxadiazol-5-il)alquil)-2-(calcogenofenil) acetamidas derivados de organocalcogênios
(Universidade Federal de Santa Maria, 2015-03-27)
In the present work, a series of 2-alkyl/arylchalcogenide-N-(4-aryl-1,3-thiazol-2-yl)acetamide was prepared via addition of aryl or alkyl chalcogenides. This methodology allowed the preparation of new derivatives of ...
Compostos de coordenação derivados do disseleneto e disselenoéteres de bis(2-piridina) síntese, caracterização e aplicações
(Universidade Federal de Santa Maria, 2015-03-06)
This work describes the synthesis and characterization of nineteen compounds derivative of diselenide and diselenoethers of bis(2-pyridyl) with metals of different degree of hardness. Among the nineteen obtained complex, ...
Síntese de novos isoxazóis e pirazóis a partir de derivados 1,3-diíno indólicos
(Universidade Federal de Santa Maria, 2015-04-06)
In this work it describe the synthesis and characterization of new 1,3-diynes indole derivatives, the 1,6-bis(1H-indol-1-yl)hexa-2,4-diynes (6 examples) and unsymmetrical 1-(5-arylpenta-2,4-diynyl)-1H-indoles (6 examples), ...