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Itens para a visualização no momento 21-30 of 30
Síntese de 2-Benzil(metil)tio-6-aril(metil)pirimidinas-4-carboxilato de Etila e seus Ácidos Derivados
(Universidade Federal de Santa Maria, 2012-08-10)
This work presents a simple and versatile synthetic strategy for the preparation of a novel series of Ethyl 2-Benzyl(methyl)tiopyrimidines-4-carboxylate 6-substituted and their acids derivatives.
The Ethyl 2-Benzyl(meth ...
Síntese one pot de 1,3,4-oxadiazóis derivados de L-aminoácidos e benzoil-hidrazidas
(Universidade Federal de Santa Maria, 2012-07-20)
In the following work, a range of 1,3,4-oxadiazles 2,5-disubstituted 3 was
prepared, using a one pot approach, from L-amino acids 1(a-e) and 2-benzoylhydrazides,
using POCl3 as dehydrating agent.
The study involved the ...
Síntese, análise estrutural e aplicação de novos complexos de Manganês como miméticos da SOD
(Universidade Federal de Santa Maria, 2012-01-15)
This work presents an study related to the synthesis and structural analysis of manganese complex with ligands of bases Schiff type, derivate from pyridoxine. Was used like starting material for the synthesis of ligands ...
Determinação de disruptores endócrinos em filé de peixe utilizando QuEChERS modificado e GC-(TQ)MS/MS
(Universidade Federal de Santa Maria, 2012-02-27)
Endocrine Disrupter Compounds (EDCs) like pesticides, alkylphenols and hormones
among other classes of compounds are responsible for alterations in the endocrine
system functions. Endocrine disruption occurs when EDCs ...
Determinação de boro em amostras de carbeto de silício utilizando piroidrólise e ICP-OES
(Universidade Federal de Santa Maria, 2012-12-13)
In this work a procedure for boron determination in samples of silicon carbide by pyrohydrolysis and detection by inductively coupled plasma optical emission spectrometry was developed. The silicon carbide samples were ...
Síntese de Pirimidinas derivadas de 7,7,7-trialo-4-metoxi-6-oxo-4- heptenoatos de metila e bi-heterociclos trifluormetilados
(Universidade Federal de Santa Maria, 2012-02-27)
An efficient method to obtain pyrimidinones and pyrimidines trialomethylated from the cyclocondensation reaction of compounds of methyl 7,7,7-trihalo-4-methoxy-6-oxoheptenoate
with urea and differents amidines providing ...
Síntese de 3-alcoxiacrilamidas a partir de tricloroacetil enol éteres
(Universidade Federal de Santa Maria, 2012-02-24)
This work reports a effective method for the preparation of a series of the new
3-alkoxy acrylamides of general formula R3HNC(O)CR1=CR2(OR), where R/ R1/ R2 =
Et/H/H, Me/H/Me, -(CH2)2-/H, -(CH2)3-/H; R3 = Allyl, n-Pr, ...
Síntese de 1,2,4-oxadiazóis derivados de 4-tiazolidinonas e arilamidoximas
(Universidade Federal de Santa Maria, 2012-07-20)
The current work reports the incorporation of 4-thiazolidinones to oxadiazolic
ring by a simple and effective methodology.
Five species of thiazolidinones were synthesized by three component
condensation reaction of ...
Desenvolvimento, otimização e validação de método rápido para determinação de ácido fólico em farinha de trigo enriquecida
(Universidade Federal de Santa Maria, 2012-03-09)
In order to eliminate the problems related to deficient intake of vitamins folate class, many food products are being subjected to the enrichment process. Among them, all types of wheat flour must be enriched with folic ...
Influência dos parâmetros reacionais na N-alquilação de 3,5-dimetil-1H-pirazol sob irradiação de micro-ondas
(Universidade Federal de Santa Maria, 2012-02-27)
This work describes the reaction parameters influence in the 3,5-dimethyl-1H-pyrazole N-alkylation under microwave irradiation. The experiments were performed in different conditions with the purpose of verified the influence ...