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Síntese de novas azinas trifluormetil substituídas e derivados a partir de reações de heterociclização de trifluoracetil enol éteres com diamino arenos
(Universidade Federal de Santa Maria, 2013-12-13)
The present research describes the study of synthetic strategies for obtaining of polyheterocyclic systems trifluoromethyl substituted from simple precursors: 4-alkoxy-1,1,1-trifluoroalk-3-en-2-ones (1), of formula ...
Síntese de Calcogenofenos e Isoquinolinas via Reações de Ciclização Intramolecular
(Universidade Federal de Santa Maria, 2013-11-26)
In the first part of this work, a series of selenophenes and tellurophenes were prepared starting from of (Z)-chalcogenoenynes, by employing FeCl3 diorganyl dichalcogenide-mediated intramolecular cyclization. In general, ...
Método multirresíduo para determinação de micotoxinas em vinho por UPLC-MS/MS
(Universidade Federal de Santa Maria, 2013-01-08)
A fast multimethod using liquid chromatography tandem mass spectrometry (UPLC-MS/MS) was implemented and optimized to yield a complete determination of 36 mycotoxins in wine samples. Extraction was performed with acetonitrile, ...
Determinação de enxofre em amostras de grafite flexível por ICP OES utilizando piroidrólise como preparo de amostra
(Universidade Federal de Santa Maria, 2013-07-16)
The flexible graphite is a material produced from the intercalation, exfoliation
and compression of graphite. Due to its low porosity, high chemical and thermal
resistance, the flexible graphite is used in many different ...
Síntese de 1,2,4-oxadiazóis 3,5-dissubstituídos derivados de Laminoácidos e arilamidoximas sob irradiação de micro-ondas
(Universidade Federal de Santa Maria, 2013-02-28)
Here we report the synthesis and characterization of 3,5-disubstituted 1,2,4-oxadiazole 3 derivatives of N-protected L-amino acid 1 and arilamidoximas 2, and the reaction was performed in a microwave reactor, using water ...
Decomposição assistida por radiação micro-ondas e ultravioleta para posterior determinação de níquel, vanádio e enxofre em coque de petróleo
(Universidade Federal de Santa Maria, 2013-07-12)
The presence of Ni, V and S in petroleum coke is undesirable because can cause poisoning in catalysts used in refining processes and problems during the coke burning such as SOX emissions, abrasion and fouling of the ...
Emprego DAETV-ICP OES para a determinação de impurezas inorgânicas em produtos farmacêuticos
(Universidade Federal de Santa Maria, 2013-03-01)
In this study a method for As, Cd, Cr, Cu, Mn, Mo, Ni, Pb, Pd, Pt, Rh, Ru and V determination in pharmaceuticals products by electrothermal vaporization inductively coupled plasma optical emission spectrometry (ETV-ICP ...
Determinação de halogênios por cromatografia de íons e ICP-MS em sulfato de bário após decomposição por piroidrólise
(Universidade Federal de Santa Maria, 2013-02-28)
In this work pyrohydrolysis is proposed as pretreatment of barium sulfate and subsequent determination of F, Cl, Br and I by ion chromatography (IC) and inductively coupled plasma mass spectrometry (ICP-MS). After the ...
Síntese de 4-trifluormetil-5-(propan-1-ol-3-il)-1H-piridin-2-iminas N-substituídas
(Universidade Federal de Santa Maria, 2013-03-08)
This work presents a simple and accessible synthetic route for the
preparation of a series, of nineteen new N-substituted 4-trifluormethyl-5-
(propan-1-ol-3-yl)-pyridin-2-(1H)-imines, obtained from the reaction between ...
Síntese de novos sulfetos, sulfóxidos e sulfonas vinílicas derivados do N-fenilpirazol
(Universidade Federal de Santa Maria, 2013-03-01)
Não foi possível inserir o abstract.